Melting point determination begins at a predefined temperature relative to the desired melting point. Up to the start temperature, the heating stand is preheated.
1. Press the open back of a capillary tube into the solid instance.
2. Invert the tube and dab gently to move the solid to the base of the capillary.
3. Place the laden tube into the hole in the melting point device, and heat at 10 degrees per minute.
4. Obey the material through the entire melting process to get a rough calculation of the melting range.
5. Turn off and let to cool by 15 degrees.
6. Return the existing tube with a new sample.
7. Heat at 2 degrees per minute via the expected range.
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